Synthesis of Ordered Cage-like Mesoporous Aluminosilicates from Na-A Zeolite Precursors Dissolved in HCl
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High-Temperature Synthesis of Ordered Mesoporous Aluminosilicates from ZSM-5 Nanoseeds with Improved Acidic Properties
Ordered mesoporous SBA-15 analogs with different Si/Al ratios were successfully prepared in a two-step process from self-assembly of ZSM-5 nanoseeds at high temperature in mildly acidic media (473 K, pH 3.5). The obtained products were characterized as SAXS, XRD, N₂ sorption, FTIR, TEM, NH₃-TPD, AAS and ICP. The results show that the initial Si/Al molar ratio of ZSM-5 precursors strongly affect...
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Highly ordered hexagonal mesoporous aluminosilicates (MAS-5) with uniform pore sizes have been successfully synthesized from assembly of preformed aluminosilcate precursors with cetyltrimethylammonium bromide (CTAB) surfactant. The aluminosilicate precursors were obtained by heating, at 100--140 degrees C for 2--10 h, aluminasilica gels at the Al(2)O(3)/SiO(2)/TEAOH/H(2)O molar ratios of 1.0/7....
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Zeolites are crystalline inorganic porous materials formed by TO4 tetrahedra (T=Si, Al, P, etc.) with ordered microporous structures. As a result of their tunable acidities and framework structures, zeolites have been used widely in catalysis and molecular adsorption/separation as well as several other emerging applications. However, the pore size of a zeolite is usually smaller than 2 nm, whic...
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تاریخ انتشار 2017